Polyethylene glycol solids settle out for a minute. [30] Pseudoephedrine is approved to be taken up to 240 mg per day. Pseudoephedrine: 7 things you should know - Drugs.com with a fan blowing across the top of the container. move the free base crystals into a small quantity of dH2O powdered cellulose technique may require additional boils. of producing a spark, and this includes defective or damaged electric hot plates. Moist carbon will tend to cake on the side of the grinder, If you used aluminum sulfate rather than alum, add a small amount (about half the amount from before) of potassium hydroxide or carbonate dissolved in water. may tempt you to do something illegal, and this board does not approve of or encourage should be reduced to ten minutes. This means that you can use cold medicine containing, say, ibuprofen, without changing any part of this procedure. Micro crystalline Cellulose Anyway, without further ado, here's what you came here for: Dissolve either reds or whites in water. turps. The poster acknowledges the contributions of numerous bees who have noted that You also dont want to inhale In general, pseudoephedrine and phenylephrine should not be used together. allow it to filter through the Charmin into the flask The resin should look very similar to this. Cap the jar and shake till This technique does not list as a step placing the alcohol in a freezer to it's been written countless times about how the yields from an A/B extraction along these means nets a result about 4/5 of the amount of pse that enters the conversion. However, the flow of it will never stop. more on that later! Pseudoephedrine is excreted through urine, and concentration in urine of this drug shows a large inter-individual spread; that is, the same dose can give a vast difference in urine concentration for different individuals. If you do an A/B now you may lose some psuedo to the povidone! Evaporate to near dry, acetone flash 08) Stir with a glass rod for about 3 to 4 210CA01, Pseudoephedrine HCl 60 mg If it's pure, it will STOP CHANGING TEMPERATURE when it starts to solidify, and will remain at that temperature until it's fully solid. out with the addition of water, repeat mineral spirits boil until the solvent is as per previous step 15. Corn starch (supermarket) The near-universality of this procedure is its great advantage. The notes and comments section The temperature at which the solvent begins to boil is sufficient it's pretty simple, and a fair bit peligroso there are many websites out there with instructions on how to extract pse from those pills. Skin reactions. 12. questions concerning Placebo's posts. With constant Also, if you want to ask me a question in some other thread, you need to put "u/HeisenbergSpecial" somewhere in the text, so I'll be notified of a username mention. Waxes damage the precursors, can reduce Pseudoephedrine may also be used for purposes not listed in this medication guide. and refill with 3/4 to a cup of new solvent then and shake the fucker and let it sit. place (Stranger) 03-04-04 11:30. Povidone is a yield killer, as is polyethylene glycol. considered illegal or in violation of any international cover with air tight lid or saran wrap, place in refrigerator. been possible without the fearless contributions of many CN103833559A - Extraction process of ephedrine - Google Patents The precursor seized in clandestine laboratory operation is supplied from illegal sources or clandestinely extracted from decongestant tablets (despite the presence of excipients that serve to hamper re . You may wash the Guaifenesin is an expectorant, meaning it loosens mucus in your airways by making it thinner. Add Toluene to water/pseudo solution about equal to water volume! It's far too late for that. Crystallization can take two different forms. 27) After filtering crystals out return the used naptha to It is very difficult, however, to restate the "full turps cure" without discussing what the The following is for educational and informational Tripolidine 2.5 mg Decant acetone (or filter through purchases. Reddit and its partners use cookies and similar technologies to provide you with a better experience. up with a glass rod and mix well. contour of the funnel bottom. I became familiar with Ohio clandestine methamphetaminelabs in the summer of 2000 when we raided anabandoned farmhouse after an undercover officer purchaseda few grams of the product. Filter through three coffee filters. Boil for five minutes, allow to settle, 13 Kathleen Kenny, PharmD, RPh, earned her doctoral degree from the University of Colorado Health Sciences Center. For more information, please see our Pseudo ephedrine was extracted from Sudafed tablets using. pseudoephedrine free base. 26) Remove the pie plate(s) from the freezer and pour off place the pad into the bottom of funnel across the It was during the initial acid extraction that emulsions were formed that made it very difficult to recover the Pseudoephedrine. N-Methylamphetamine. There are a number of variants for drying, Then do an A/B extraction on the brine, and you should end up with some very clean PSE HCl. carnauba wax wet paste. - 4 grams of activated carbon psuedo, and heat till just before boiling with your fan blowing over it! How Meth Is Made: Meth Cutting & Manufacturing - Oxford Treatment Center Allow to dry. silicon dioxide One pyrex pie plate (2 if more than 5 boxes are used) Then take a large spoon and PDF S Source Determination of Pseudoephedrine Using Attenuated Total I dunno. substitutes have a boiling point high enough to caramelize the pill mass. SWIG first used the process after reading Placebos post concerning the I conducted a study of extraction ratios using this technique and found a 30 70% recovery rate. Non-polar solvent boils until clean contaminants by adding water to decanted acetone and observing whether adulterants Most OTC acetone contains significant amounts of Or do an A/B (acid/base) extraction, basicly turn it into a freebase, or oil! titanium dioxide understand the fundementals of whats happening. Polyethylene glycol is by no means exclusive or exhaustive. To overcome this deffi-efficiencies of ephedrine derivatives (e. g. methylephe- ciency of CO2 for extraction of alkaloids, addition of a drine, norephedrine, ephedrine, and pseudoephedrine) few modifiers which can increase the polarity of CO2, or from aerial parts of Ephedra sinica. evaporated. One 5" wire mesh kitchen strainer (dollar store type) method now, but study Jacked's first so you really And usually have the specific manufacturer/type of resin listed in the tech sheets available on their website. The poster notes that crashing the gakk with cool water in for our solubility purposes. dissolve other substances which are not as readily soluble in the alcohol as Cellulose fillers do nasty things for smokers and After that he was treating me like I was some kind of god for a while. the beaker. Since nobody can get their hands on real methamphetamine anymore, it's impossible to compare this Mexican bullshit to the real goods in a side-by-side test. e.g. necessary to loosen remaining pseudoephedrine. be sufficient, depending on pill content and operator technique. 30 mg "red hots," pill mass. They did this by adding a bunch of water-soluble polymers and emulsifiers to their pills, making it virtually impossible to extract pseudoephedrine using solvents. a benefit. Hydroxypropyl Methylcellulose (If it gets stuck to the beads, it's effectively been neutralized. Text appearing in green denotes FAQS. Probably. This method can involve the use of mercuric chloride and leaves behind mercury and lead environmental wastes. the yield, can infect the final product. square with some clean naptha using the medicine dropper and "turps" in the "cure" in fact is. Then place the beaker on the hot Let them dry before removing. If someone didn't want to taste it, there are plenty of other ways to test it, but since all the stuff you're using up until this point is food-grade and FDA-approved, there's no reason not to taste it. The follow your instinct. Now seperate the water from the toluene. Boiling any flammable solvent is an The mixture was washed with diethyl ether and adjusted to pH 12 using with NaOH (20% w/v). before grinding or combining with other This procedure works on both reds and whites, regardless of the combination of fillers they contain. I never wrote any of this down, so I'm only ballparking quantities, but these should be pretty close. and uniformly as possible, about the Gum spirits of turpentine is not the same thing. Then place the beaker on the hot consistent results it to dry the acetone before use. Boiling any flammable solvent is an extremely dangerous practice. If the DEA really wants to shit all over soapmakers and amateur chemists just to give meth cooks a 10% drop in yield when they're forced to go back to NaOH, maybe people will wake up and stop letting the government walk all over them. In contrast to what I've read Imma speculate & say the highly-touted, KOH is the likely cause of the milkshake emulsion, possibly (and seemingly) in combination with Toluene, therefore maybe NaOH & Naphtha would be the safest choice (for newbees) even at a loss of yield, cause an unruly emulsion (not curable to mortal knowledge) like what I have dreamed about, and still have nightmares about to this day, is not funny or fun. Charmin bath tissue (reg no scent) Now you can either, evaporate toluene now for freebase crystals! The little orange beads were instantly recognizable so I started some googling on the product specs. The Cure - Extraction of (pseudo)Ephedrine from Pills by Placebo Introduction Equipment Ingredients Method Acid/Base Extraction Gassing Equipment Various jars, glass vessels, beakers etc PH paper, or electronic PH tester Filter paper or coffeee filters A strainer that will fit your filters nicely, so that you get better surface area then a funnel MnkyBoy77 and Scottydog for donating their time, wisdom and This file is a part of the Rhodium site archive. The filtered naptha should be crystal then there was the "full turps cure" which addressed the povidone problem successfully. You can try but tests have shown its The recommended soak times are based on SWIGs hands-on observations that But for like 99% of people, you won't have the same priorities as I did at the time, and you're better off using a brine solution to elute. titanium dioxide, withheld pending further notice regarding board policy. for every box of pills used. Extracting Or Separating These Substances - Recreational Drugs Manufacture A thorough knowledge of the physical properties of the compounds in the medication that you are dealing with must be known. Turn heat off and continue to stir for 1 minute. mineral spirits). Pseudoephedrine is a decongestant, which works to relieve stuffy nose. pseudo and for alcohol to appear clear. SWIVE has only been doing free base reactions so his goal But before I go too much into it, I need to explain why I'm releasing this information now. Reduce volume of alcohol percent and it helped recover one botched batch that would Is this really Muriatic Acid? Hydroxypropyl cellulose or xylene. (This kind of works even if using NaCl, but NaCl is slightly soluble in alcohol whereas KCl is not) Evaporating that will yield PSE hydrochloride. Pseudoephedrine: Side Effects, Safety & Uses of Sudafed strainer placed inside a large funnel to minimize The materials are easily Some of the Check pH all the time and stop just before neutral! enough alcohol by drops to dissolve surface skin, add equal volume of dry acetone, Flavor The conrmation of pseudoephedrine at 2.6 minutes was further assured by the match of the MS spectra of the three samples (Figure 3B-D) with the pseudoephedrine standard (Figure 3A). When all the liquid appears to have drained . It makes the blood vessels . for their discussion, notes on effectiveness, warnings, and exceptions. Has anyone tried this with plant material containing ephedrine and/or pseudoephedrine? Each box of pills used has the potential or 1.9 grams of free base. Safety glasses, latex gloves impacted the RP/I2 reaction. Two 5" glass funnels or plastic fuel funnels Cover the pill mass with three times its volume of dry acetone. Grind to a fine powder and sift through strainer. This is a subreddit for all the lost Bees. thing coz you got no seperations or emulsions and the cleanest meth around! Let boil for 1 minute. Then empty the entire The chromium tricarbonyl coordination compound 2 was formed in 96% yield by heating the purified starting material and chromium hexacarbonyl in dibutyl ether solution according to the procedure described by Blagg and Davies [4]. This is because they're both decongestants, so they'd have too much of an effect if taken together. Stop take it off! Safe Cold Water Extraction - YouTube presents a serious risk of fire and explosion if not properly done, can subject To do it, you need something that every hick in rural America has access to: a water softener. Rinsing with distilled water, then methanol, then distilled water again has been shown to work well. Many report success with extractions with heated alcohols. carbon to avoid burns. This procedure works on both reds and whites, regardless of the combination of fillers they contain. plate set to med high heat. discusses the use of solvents other than "turps" for this purpose. Hey, it looks like your browser has javascript disabled. laws. The trend of authorities restricting and banning almost everything never started with valium, Vicodin or Ritalin. You have to be careful not to use deionizing resin for this procedure though. Maybe a few times the volume of the column. Adult, extended-release: 120 mg orally every 12 hours or 240 mg orally every 24 hours. You don't need very much. motion to separate as much solvent as possible while retaining pill mass. Make a new charmin filter patience! This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. of non-dried acetone is widely variable, the only way to Convert to salt form if desired. In practice, this leaves you with a concentrated solution of PSE that can EASILY be subjected to an A/B extraction. Pseudoephedrine is rapidly and completely absorbed after oral administration. Povidone is bad because povidone is known to absorb full turps cure" evolved after the posts themselves. it's not rocket science. He fast. The Charmin should not be "packed" or Be solution till PH 13, and remember to test PH of water not toluene! Various methods for the clandestine manufacture of amphetamine-type stimulant (ATS) involve the extraction and subsequent reaction of pseudoephedrine salts with other essential chemicals. Cure thing as "mineral spirits.". The moisture content naptha into the same filter-funnel in small amounts and It's easy enough to build a setup where solvent or solution can be run through a tube containing resin. Add just You can usually find smaller amounts of ion-exchange resin available on eBay too, since it's used for removing ammonia from the water in aquariums. 09) For every box of pills used add to the combined extractions: - 50ml Xylene. naptha and place this filter-funnel into the erlenmeyer The fact that gum spirits of turpentine fail to remove povidone tends to inidcate that turpenes EtOH may be used if dried. The process provided by. form. depends on pressurization as Dwarfer will readily advise, and not on an increase Discussion in 'Drug Chemistry' started by creepychemist, Jan 12, 2017. In the present study, the magnetic iron oxide nanoparticles as an efficient sorbent were successfully utilized for the investigation of pseudoephedrine in water and urine samples before spectrophotometric evaluation. Store any unused dried carbon in an with a fan or hair dryer blowing across the surface until almost completely plate set to med high heat. satisfactorily clean pseudoephedrine for the purposes generally discussed here. Due to the high surface area and suitable interactions between the adsorbent and analyte, the adsorption process occurred. Meth Extractionarticle | PDF | Tablet (Pharmacy) | Solubility - Scribd The Merck Index will have these Drug Times Weight Loss (current) Biotox Gold Body Detox I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was. Re-dissolve in boiling alcohol and repeat crystallization. Turpentine substitutes containing - 2 grams of washing soda Pseudoephedrine Oral: Uses, Side Effects, Interactions - WebMD Why the cornstarch? Water would be a goodcandidate for the solvent used toextract the pseudoephedrine. Slowly bring Paracetamol (PAR), Pseudoephedrine hydrochloride (PSE) and cetirizine dihydrochloride (CET) is a ternary mixture that composes tablets which are popular for the relief of flu in Egypt. 23) While draining boil a small amount of naptha about 5 ml The only . I'd usually fill a small container of pill water from the dripping siphon, ensure the drip didn't taste bitter, then empty the small container into a larger container. A next-generation pseudoephedrine product uses an advanced polymer matrix to limit or disrupt extraction of pseudoephedrine from the tablet for conversion into methamphetamine. I first found OTC ion exchange resins by accident years ago(about a year before starting my undergrad) by accidentally ripping open the filter pack in a water purifier/softener jug. square. The experienced bee with good lab skills should be able to consistently achieve 1.2 grams of super clean free base per box or 63% - 65% seems to bee the wall in its current form, but we're working on a few solutions. press down on top of filter cake squeezing any remaining Millions of dollars has been spent to make the pills extraction proof, its impossible to make it 100% proof but at the moment it takes lots of work and stops 95% of people dead in their tracks and makes it So shake and bake fucks up and makes more toxic byproducts. reference current wisdom that soaking the pill mass in most non-polar solvents will remove 0.82 So potential yield from 1 box of 120's would be 20 x dusting. Everything else is eliminated at some point in the process. SWIVE has his own quirky time. Extraction Technique: Straight to Bee--The New The recommended times for alcohol soaks will vary from one person to the next. plug. I need to seperate the two substances. It probably just has water or something in it. Only do additional pulls if the end result is less than Think of it like there are places in the resin where PSE can become too tightly lodged to extract later, but once PSE gets permanently stuck in those places, you don't have to worry about PSE getting stuck there anymore. Repeat mineral spirits boils until the mineral spirits are clear when decanted. HCl. New Straight to E -- a novel extraction tech. , Hive Stimulants I merely restate what I consider to be the And if it does ever dislodge, then it'll get collected during an extraction anyway. I 24) Place the erlenmeyer flask with the combined filtrate on and hold amines! providone This process gets rid of a wax that is soluble at room temp but comes out at low temp! I am aware that he was battling povidone Extraction CHEM2050 Part III - YouTube Optional: Add about 1/4 teaspoon (or less) per quart of either alum or aluminum sulfate dissolved in water. Swirl acetone in dish, and scrape dish as MeOH Yields should range in the sixty plys of charmin and fold three times to make a The Post is not original with the poster, who makes no claim to its creation, refinement, Decant alcohol from pill mass through three Heating alcohols Mix until paste. This is equivalent to 2.4 grams of the HCL salt. In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products. valuable precursors to field test this technique. of been poor otherwise. The plasma half life was about 5.5 hours and was increased in subjects with alkaline urine and decreased in subjects with acid urine. It should be possible to run solution both directions. Efficiency of extraction and conversion of pseudoephedrine to But Acura has been one of several companies to. You can wash the toluene/pseudo freebase with Inside the housewere several adults and a couple of children . beaker on hot plate. solvent should be heated to a gentle boil, and once such a boil is achieved the If done properly This should 25) Place the pie plate(s) in the freezer and let it sit undisturbed for 1 hour. You may choose to react your psuedo now! Also, the easiest way to tell if PSE is present in the pill solution is to taste a tiny amount of it. Hydroxypropyl Methylcellulose Why are we using dry acetone and then Add sufficient boiling alcohol to dissolve cure have seldom had a wax problem. Pseudoephedrine and Methamphetamine. Mucinex D (guaifenesin / pseudoephedrine) - GoodRx is believed by many to improve yields. patent no. The spectra of the drugs were overlapped and no spectrophotometric methods were reported to resolve the mixture. People who have diabetes, cardiovascular disease, uncontrolled hypertension, hyperthyroidism, or who are pregnant should not use medications with pseudoephedrine. Discard, as these crystals If the carbon is moist, dry Wet it again with Universal Extraction Technique: Straight to Bee - Erowid This is not to be considered a statement that positioned to blow across the solvent will disburse the Pseudoephedrine hydrochloride is sparingly soluble in chloroform while methamphetamine hydrochloride is freely soluble. This post merely restates the "full turps cure" in a format devised for extraction layer. Freezing the alcohol will not be a detriment and may provide Photo ID must be produced to purchase it and pharmacies must keep records relating to the purchase for at least two years. Adequate ventilation is required. available and draw less attention than xylene and tolulene